Automated, parallel library synthesis in verasatile 96-well plates with disposable glass vials / reactors under accelerating superheated conditions (van't Hoff rule).
OVERVIEW
Chemspeed's solution
The FLEX SPEEDCHEM uses a combination of elevated temperature and autogeneous pressure to dramatically increase the reaction rate, resulting in shorter reaction times and often higher selectivities for e.g. small-molecule, polymer, porous materials, cathode materials synthesis.
WORKFLOW
Example workflow
The interactive workflow panel below showcases example workflows for this solution. Each Chemspeed tool or module performs a set of specific actions, as in any manual lab workflow, and an almost limitless arrangement of these tools is possible.
BENEFITS
Powerful advantages
Ventilated hood for safety and trolley.
Optimized footprint (3x3 ft, 90x90 cm) versus capacity - all while reducing costs and maximizing return on investment.
Increased temperature to e.g. 40°C above the boiling point results in about 16 times faster reaction at better quality.
Reagent preparation (liquids and solids), multistep synthesis, work-up, purification, analysis and product transfer to storage.
Disposable glass reactors in versatile MTP format.
4-Needle Head for volumetric liquid handling and sampling.
Gravimetric solid dispensing into an unlimited choice of vial / plate / reactor formats.
Powder dispensing / dosing robotic tool can be combined with other tools to accommodate multiple workflows.
Higher reagents solubility into solvent.
Milder reaction conditions.
Less side reactions / reagent alteration and higher chemical yield.
Lower energy usage.